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Some previous work by one of the authors with wires of an alloy of platinum-iridium, portions of which work were published in these Proceedings, indicated that when the wires were used as suspensions for torsion pendulums, the relations between the period of vibration and the amplitude were exceedingly complicated. The effect of drawing these wires was dealt with in another paper. In all these papers referred to, the statement was made that similar tests should be applied to some of the more common wires in the hope of finding similar, even though smaller effects. Through press of work these experiments have been deferred until the present year. This particular paper will deal with but one feature of the work, namely, the effect of drawing on the elastic nature of phosphor bronze wires. The writers are indebted to the American Electrical Works, of Phillipsdale, Rhode Island, for kindly furnishing them with specimens of the wires.
- the evidence filed by the Appellant in support of an alleged prejudice against the use of a DOC in combination with a diesel fuel comprising a platinum group metal compound did not convincingly prove that such a prejudice existed at the priority date of the present application;
submitted provisionally inter alia that document (3) disclosed a method for reducing the emissions from the exhaust of a diesel engine equipped with a DOC by means of a diesel fuel comprising specific platinum group metal compounds and was thus more relevant than documents (1) or (2) for the evaluation of inventive step of the claimed subject-matter.
introducing a fuel comprising a platinum group metal composition into a combustion chamber of a diesel engine, said platinum group metal composition being stable in the fuel composition prior to combustion and consumable during combustion to release platinum metal catalyst in active form; and
"an additive containing a platinum group metal compound and a cerium, iron and/or copper compound into a combustion chamber of a diesel engine, said platinum group metal composition being stable in the fuel composition prior to combustion and consumable during combustion to release platinum metal catalyst in active form, and the additive comprising a platinum group metal compound soluble in the diesel fuel which is added in amounts effective to provide concentrations of the metal in the fuel of less than 1 part per million (ppm) and said cerium, iron and/or copper compound in amounts effective to provide concentrations of cerium, iron or copper metal in the fuel of from about 1 to about 100 ppm or a platinum group metal compound dispersible in a fuel-water emulsion, said platinum group metal compound being added in amounts effective to provide concentrations of the metal in the fuel of less than 1 part per million (ppm) and said cerium, iron and/or copper compound being added in amounts effective to provide concentrations of cerium, iron or copper metal in the fuel of from about 1 to about 100 ppm;"
The only claim according to the second auxiliary request differs from the claim according to the first auxiliary request insofar as the used fuel must comprise an additive comprising a platinum group metal compound and a cerium compound, the wording between "introducing a fuel comprising" and "combusting the fuel..." reading then as follows:
"an additive containing a platinum group metal compound and a cerium compound into a combustion chamber of a diesel engine, said platinum group metal composition being stable in the fuel composition prior to combustion and consumable during combustion to release platinum metal catalyst in active form, and the additive comprising a platinum group metal compound soluble in the diesel fuel which is added in amounts effective to provide concentrations of the metal in the fuel of less than 1 part per million (ppm) and said cerium compound in an amount effective to provide a concentration of cerium metal in the fuel of from 1 to 30. ppm or a platinum group metal compound dispersible in a fuel-water emulsion, said platinum group metal compound being added in amounts effective to provide concentrations of the metal in the fuel of less than 1 part per million (ppm) and said cerium compound being added in an amount effective to provide a concentration of cerium metal in the fuel of from 1 to 30 ppm;".
VII. As to the support of claim 1 according to the main request under Article 84 EPC, the Appellant explained during oral proceedings that the platinum metal compositions suitable for use in the claimed invention were the compositions of platinum metal group compounds, including complexes, known to be suitable additives for a diesel fuel.
- moreover, because of the existing concern about the pollution caused by the particulate emissions of diesel engines, there existed a prejudice at the priority date of the present application against the use of a DOC in the absence of a DPT able to trap metal particles for reducing the emissions in the exhaust of a diesel engine when used in combination with a fuel comprising a metal catalyst such as platinum, as shown e.g. in the Exhibits (ii), (iii) and (AA) through (KK);
- as shown in Exhibits (D) through (I) and in the experimental report filed under cover of the letter dated 28 February 2005, the claimed invention provided unexpectedly a high removal of particulates and of other gaseous emissions, including NOx, from the exhaust of a lean-burn diesel engine; in particular, the use of a fuel containing a combination of a platinum group metal and a cerium compound provided a reliable and constant reduction of the particulate matter above the 25% reduction obtainable by means of a DOC alone and at and above the threshold of 30% reduction and also a reduction of the NO2 contained in the emitted NOx which was not possible to achieve with a fuel containing only a platinum metal compound;
- moreover, because of the similarities of iron and copper metals with cerium, the same effect obtained by means of a fuel containing a combination of a platinum group metal compound and a cerium compound had to be expected with a fuel comprising a combination of the platinum group metal compound with an iron or copper compound. 2ff7e9595c
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